NMR-spin-echo study of pinning of domain walls in cobalt micropowders, nanopowders and nanowires
DOI:
https://doi.org/10.3103/S0735272723080058Keywords:
nuclear spin echo, magnetic video pulse, single-pulse echo, double-pulse echo, cobalt, pinningAbstract
The pinning of domain walls in cobalt micropowders, nanopowders, and nanowires is studied by the double-pulse spin-echo NMR method under an additional magnetic video pulse. Cobalt micropowders are obtained by melting in an induction furnace. Nanopowders are produced using electron beam technology and chemical deposition. This chemical deposition reaction is carried out in an external magnetic field to obtain nanowires.
The pinning in these systems is measured as a function of the long-term magnetic video pulse and its amplitude. It is established that the magnetic video pulse area is constant for all its threshold values corresponding to the beginning of the double-pulse echo signal suppression. The linear nature of the pinning dependence on the external magnetic field magnitude in cobalt micropowders in a wider range of the external magnetic field change compared to lithium ferrite is presented. Alternative information about the pinning strength of domain walls in magnets can also be obtained by studying the magnetic video pulse influence on the magnetic echo signal formed by the joint action of radio frequency and magnetic pulses. These NMR methods can be used for microscopic control of the domain wall properties in the studied magnets with the aim of their potential use in functional materials, memory devices, and sensors.
References
Е. А. Turov, М. P. Petrov, Nuclear magnetic resonance in ferro- and antiferromagnets, [in Russian]. Moscow: Nauka, 1969.
S. Wurmehl, J. T. Kohlhepp, “Nuclear magnetic resonance studies of materials for spintronic applications,” J. Phys. D Appl. Phys., vol. 41, no. 17, p. 173002, 2008, doi: https://doi.org/10.1088/0022-3727/41/17/173002.
A. A. Shmyreva, V. V. Matveev, G. Y. Yurkov, “Nuclear magnetic resonance in magnetic nano-materials as an effective technique to test and/or to certificate local magnetic properties,” Int. J. Nanotechnol., vol. 13, no. 1/2/3, p. 126, 2016, doi: https://doi.org/10.1504/IJNT.2016.074527.
I. V. Pleshakov, P. S. Popov, Y. I. Kuz’min, V. I. Dudkin, “NMR study of domain wall pinning in a magnetically ordered material,” Tech. Phys. Lett., vol. 42, no. 1, pp. 59–62, 2016, doi: https://doi.org/10.1134/S1063785016010296.
T. Gavasheli, T. Gegechkori, G. Mamniashvili, G. Ghvedashvili, “NMR spin echo study of domain wall pinning in lithium ferrite in combination with an additional magnetic video-pulse,” in 2021 IEEE 26th International Seminar/Workshop on Direct and Inverse Problems of Electromagnetic and Acoustic Wave Theory (DIPED), 2021, pp. 199–202, doi: https://doi.org/10.1109/DIPED53165.2021.9552256.
J. K. Galt, “Motion of individual domain walls in a nickel-iron ferrite,” Bell Syst. Tech. J., vol. 33, no. 5, pp. 1023–1054, 1954, doi: https://doi.org/10.1002/j.1538-7305.1954.tb02363.x.
L. А. Rassvetalov, А. B. Levitskii, “Influence of pulsed magnetic field on nuclear spin echo in some ferro- and ferrimagnets,” Phys. Solid State, vol. 23, no. 11, pp. 3353–3359, 1981.
G. I. Mamniashvili, T. O. Gegechkori, T. A. Gavasheli, “A study of the nature of the NMR signal in lithium ferrite upon exposure to a low-frequency magnetic field,” Phys. Met. Metallogr., vol. 122, no. 9, pp. 841–846, 2021, doi: https://doi.org/10.1134/S0031918X21090088.
T. Khoperia, G. Mamniashvili, M. Nadareishvili, T. Zedginidze, “Competitive nanotechnology for deposition of films and fabrication of powder-like particles,” ECS Trans., vol. 35, no. 10, pp. 17–30, 2011, doi: https://doi.org/10.1149/1.3640401.
D. Japaridze et al., “Magnetic properties and photocatalytic activity of the TiO2 micropowders and nanopowders coated by Ni nanoclusters,” J. Supercond. Nov. Magn., vol. 32, no. 10, pp. 3211–3216, 2019, doi: https://doi.org/10.1007/s10948-019-5088-2.
T. Gavasheli, G. Mamniashvili, G. Ghvedashvili, T. Gegechkori, “NMR spin-echo study of the domain wall pinning in cobalt micropowders,” in 2022 IEEE 2nd Ukrainian Microwave Week (UkrMW), 2022, pp. 405–409, doi: https://doi.org/10.1109/UkrMW58013.2022.10037055.
G. I. Mamniashvili, T. O. Gegechkori, “Investigation of the characteristics of domain wall fixation centers in cobalt by nuclear magnetic resonance,” J. Appl. Spectrosc., vol. 89, no. 6, pp. 1076–1079, 2023, doi: https://doi.org/10.1007/s10812-023-01469-y.
P. Scholzen et al., “Magnetic structure and internal field nuclear magnetic resonance of cobalt nanowires,” Phys. Chem. Chem. Phys., vol. 24, no. 19, pp. 11898–11909, 2022, doi: https://doi.org/10.1039/D1CP05164D.
T. A. Gavasheli et al., “Investigation of the pinning and mobility of domain walls in cobalt micro- and nanowires by the nuclear spin echo method under the additional influence of a magnetic video pulse,” J. Magn. Magn. Mater., vol. 500, p. 166310, 2020, doi: https://doi.org/10.1016/j.jmmm.2019.166310.
G. Маmniashvili et al., “Production of cobalt nanopowders by electron-beam technology and their NMR and magnetometry study,” J. Magn. Magn. Mater., vol. 373, pp. 177–182, 2015, doi: https://doi.org/10.1016/j.jmmm.2014.03.058.
S. Konishi, K. Mizuno, F. Watanabe, K. Narita, “Domain wall displacement under pulsed magnetic field,” in AIP Conf Proc., 1976, pp. 145–147, doi: https://doi.org/10.1063/1.2946043.
D. Bartran, H. Bourne, “Domain wall velocity and interrupted pulse experiments,” IEEE Trans. Magn., vol. 9, no. 4, pp. 609–613, 1973, doi: https://doi.org/10.1109/TMAG.1973.1067703.
V. A. Ignatchenko, V. K. Mal’tsev, A. E. Reihgardt, V. I. Tsifrinovich, “New mechanism for formation of nuclear spin echo,” JETP Lett., vol. 37, no. 9, p. 520, 1983.